Wijs' Reagent 0.1 mol/l (0.2N) for volumetric analysis

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Name Wijs' Reagent 0.1 mol/l (0.2N) for volumetric analysis
Manufacturer Sigma-Aldrich
Volume 1 L
Molarity 0.1 mol/l
Normality 0.2N
Application Volumetric analysis
Color Brownish yellow
Solubility Soluble in chloroform and carbon tetrachloride
Storage Condition Store at room temperature
Shelf Life 2 years
Hazards Causes skin irritation and serious eye damage. May be harmful if swallowed or inhaled
Precautions Wear protective gloves/eye protection/face protection. Avoid breathing dust/fume/gas/mist/vapors/spray
UN Number 1760
UN Proper Shipping Name Corrosive liquid, n.o.s. (Iodine chloride)
UN Class 8
Packing Group II
Storage Temperature Room temperature
Product Code 247373
FAQ
What is Wijs' Reagent used for in volumetric analysis?
Wijs' Reagent is commonly used for the determination of iodine value in lipids and fats. It is also used for the titration of unsaturated compounds, such as alkenes and alkynes, in organic compounds.

How is Wijs' Reagent prepared for use in volumetric analysis?
To prepare Wijs' Reagent, a solution of iodine is added to a solution of potassium iodide in glacial acetic acid. This solution is then standardized with standard sodium thiosulfate solution to determine its exact concentration for use in titrations.

What is the concentration of Wijs' Reagent commonly used in volumetric analysis?
Wijs' Reagent is typically prepared at a concentration of 0.1 mol/L (0.2N) for use in volumetric analysis. This concentration is suitable for most titrations involving unsaturated compounds and is commonly used in analytical laboratories.

How accurate is the titration using Wijs' Reagent for volumetric analysis?
The titration using Wijs' Reagent is known for its high accuracy and precision in determining iodine value and other unsaturated compounds in organic samples. Proper standardization and handling of the reagent are crucial for obtaining accurate results.

Are there any precautions to be taken when using Wijs' Reagent for volumetric analysis?
Some precautions to be taken when using Wijs' Reagent include handling the reagent with care, as it contains hazardous chemicals. Proper disposal of waste solutions and wearing appropriate personal protective equipment are also important when working with this reagent.
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